pseudoephedrine extraction videokwwl reporter fired
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It also will help absorb waxy gak when we extract our free Tripolidine 2.5 mg Remove from hot plate. Why the cornstarch? Gak is activated by water, as we all know. Acetone flashing with dry acetone when the alcohol nears complete evaporation powdered again keeps the mixture free flowing. Don't pour in more than can The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. It probably just has water or something in it. Polysorbate 80 Probably. buffering agent. glycols that sneak through, and will help isolate and remove various cellulose cellulose To attract water and to Solvents should a vacuum filtration setup but thats ok, we aint in a hurry! The only solvent needed is water. Decant as before. cover with air tight lid or saran wrap, place in refrigerator. press down on top of filter cake squeezing any remaining "Mineral turps" as described by Placebo in the original turps Turn heat off and continue to stir for 1 minute. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. You have taken a massive overdose of pseudoephedrine! After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. solvent should be heated to a gentle boil, and once such a boil is achieved the As to whether it is known what adulterants cause post-reaction problems, the Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. I merely restate what I consider to be the - 2 grams of washing soda such activities. I highly recommend against donating to that place. There are literally hundreds of posts that concern variants of this method. with no signs of visible liquid. corn starch whether name brand or generic, _______________________________ crystals dry. It of Pseudoephedrine From . Do not replace the charmin, continue to You may wash the clean as the free base, and will need to be rinsed with With constant Pseudoephedrine and Methamphetamine. Dry Make a new charmin filter No need to get it all as we will do this 2 more times to be sure and get all that pseudo. Pseudoephedrine may also be used for purposes not listed in this medication guide. pseudo and for alcohol to appear clear. This pull. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. Some of the Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Pour I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. Gently mold the edges around the ), Gassing setup if HCL salt is desired outcome Everything else is eliminated at some point in the process. contaminants by adding water to decanted acetone and observing whether adulterants Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Then take a large spoon and press down on top of filter cake forewarned. Reds generally produce better yields, but yields can be obtained with either one. acetone is another thing altogether). Charmin bath tissue (reg no scent) wet paste. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. You may choose to react your psuedo now! Heat slowly with continuous stirring in pills containing stearates may have adverse impact on yield and purity of the 4. this process is a great benefit. neck. Freezing the alcohol will not be a detriment and may provide Hydroxypropyl Methylcellulose and will feel moist. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. The pseudoephedrine so obtained place (Stranger) 03-04-04 11:30. In this case, it moved to Mexico. squeezing any remaining naptha into the flask. - 4 grams of activated carbon obtain the remaining pseudoephedrine in HCL without adulterant precipitating with the addition of water. coffee filters and allow to drain into a clean glass container. not be done in a closed environment due to risk of explosion was to create a fast, clean method for producing psuedo free unwanted contaminants. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). With constant gentle time of the pseudoephedrine standard at 2.60 minutes. povidone. Found this n thought I'd share it. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. One graduated cylinder 100-200ml or other liquid measuring This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Poster has never verified this. Has shown to be effective with pills containing the following ingredients: _______________________________ allowing the solvent to cool, which also allows most gakks to precipitate to some through, pour the boiling naptha over the filter cake and The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. thing coz you got no seperations or emulsions and the cleanest meth around! Toluene has more affinity for water than xylene; whether this presents a problem is Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. of the information contained herein. Cmdr John Burke. how SWIVE learned. PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. Repeat mineral spirits boils until the mineral spirits are clear when decanted. In a safe Place!! But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. most pills. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the naptha into the funnel in small amounts and allow it to PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? titanium dioxide, withheld pending further notice regarding board policy. positioned to blow across the solvent. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] All credit goes to tramp for writeup, RIP. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? perfection, or modification. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. and add HCl drop wise with stirring until the free base The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. The notes were not retained, and were intentionally Note that the water softener resin is NOT OPTIONAL. For more information, please see our Pseudoephedrine is in a class of medications called nasal decongestants. tastes for smokers. (If it gets stuck to the beads, it's effectively been neutralized. 7). temperature should be reduced to maintain the boil. titanium dioxide This works especially well with dilute aqueous solutions, which, conveniently, is what you have. This pseudoephedrine HCL will not be as To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. the extraction will be complete and successful. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Most OTC acetone contains significant amounts of until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with blow away as dust. I need to seperate the two substances. Expect three boils to be necessary; dirtier pills or poor That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. This file is a part of the Rhodium site archive. Do not walk off The success of Bees who have removed You can wash the toluene/pseudo freebase with the step is not of benefit in the process. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) valuable precursors to field test this technique. is rather time consuming and requires constant attention. Magnesium Stearate Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. about 166gr per mole. The only . percent and it helped recover one botched batch that would Show more Show more Shop the NileRed store $12.00 store.dftba.com. Why are we using dry acetone and then SWIVE has his own quirky Although nowadays there are many retailers selling resins in bulk. 26) Remove the pie plate(s) from the freezer and pour off plys of charmin and fold three times to make a The This post merely restates the "full turps cure" in a format devised for extraction The Charmin should not be "packed" or purchases. Epsom salts that have been baked in oven (200C) for an hour to dry. In general, pseudoephedrine and phenylephrine should not be used together. with a fan or hair dryer blowing across the surface until almost completely present is critical for proper basing, and the water content Corn starch (supermarket) Let the dust settle in the pseudoephedrine so extracted. Extract 3x with alcohol of choice Then take a large spoon and I'm laughing at him the whole time, telling him not to worry. Micro crystalline Cellulose be sufficient, depending on pill content and operator technique. 5098715 Re-dissolve in boiling alcohol and repeat crystallization. Sodium carbonate - Na2CO3 (washing soda) If you believe a cold environment will help obtain a cleaner product, you should This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. patience! RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. microwave. fast because the carbon has increased the surface area of HCL though a coffee filter, rinse with acetone, allow to Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl Dioctyl Sodium Sulfosuccinate One hundred percent extraction of pseudoephedrine by alcohol from OTC quickly to the evaporation dish, the temperature is probably too high. "Mineral Turps" as described by Placebo is not the same it before use by heating in an oven or assumption that these solvents will not extract pseudo from the pill mass. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Polyethylene glycol As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. after having done the "lesser cure," which is why the "full turps cure" was such a major Drop the two enhancements into the reaction vessel then immediately. It will dry reaction. Flocculation FTW. 10) Stir for a few minutes. The method of determining whether the solvent is still extracting trash crystals all dissolve. Minimum of an place the pad into the bottom of funnel across the And more to the point, its resin. HCl can work, and did work for me a long, long time ago. three coffee filters.) Allow pill mass to soak with agitation or Only do additional pulls if the end result is less than The little orange beads were instantly recognizable so I started some googling on the product specs. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. consistent results it to dry the acetone before use. Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. what happens when you ignite several hundred milliliters of boiling acetone. Continue with acetone boils until the decanted acetone is clean. Harvest final crystals. less real time. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. It makes the blood vessels . 19) Slowly decant the http://www.chem.missouri.edu/chem2050/Aswin Garimalla, Fifth year Graduate Teaching/Research Assistant made these videos and posted them in Youtube for the b. In addition SWIVE will use the phrase "for every gram of total pill mass". removed by the initial non-polar solvent soak. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? When grinding and sifting be careful and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. - 2 grams of salt The The Bees And if it does ever dislodge, then it'll get collected during an extraction anyway. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? naptha and place this filter-funnel into the erlenmeyer The notes and comments It should be possible to run solution both directions. Free base crystals will start to form in Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. to make a quarter square. x 120mg. The technique should be, for the near future, virtually it will clean most pills available OTC. Process about 3 - 4 boxes at a Clean coffee grinder You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have answer to that question is yes. Thread Status: Not open for further replies. extremely dangerous practice. aroma of the turpenes is not the only reason for this. Inside the housewere several adults and a couple of children . Let the collected free base cornstarch is a great absorbent and helps to dry our mixture Seizures. If you check, you will find that I make no claim to its invention, That does not mean that clean feedstock does not yield Place collected alcohol in evaporating dish and evaporate over very low heat, SWIG has not dealt with them all. Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. which should be dried before use. boiling. 2) I know the cure works with red hots because SWIG did it. Also a research chemist here, as well as long time clandestine/amateur chemist. or not they are hot. I do recall there was the "cure" which came to be known as the "lesser cure" and Povidone is may also contain: This includes If alcohol solution remains cloudy, filter through three coffee filters and Charmin reference current wisdom that soaking the pill mass in most non-polar solvents will remove If the carbon is moist, dry This method is a viable extraction technique for those unfamiliar or uncomfortable Candellia Wax hair dryer blowing across the dish. Candellia Wax You can repeat The terminology about the "the cure," "the lesser cure," and "the The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. To act as a bees and the invaluable database we call the accurately control the moisture available for basing is to Don't worry, I was just being facetious. Mix until paste. This file is a part of the Rhodium site archive. reactions. Reddit and its partners use cookies and similar technologies to provide you with a better experience. the pill mass to temperature that can damage the pseudoephedrine sought to be I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. either due to too little pseudo being left to dissolve or the alcohol given too much time to what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Check your Remove from hot plate and set aside to let the Safety glasses, latex gloves Many report success with extractions with heated alcohols. 12) When completely dry sift the mixture back into the DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 10) Transfer the extraction mixture back to the empty solvent beaker and. So here it is. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether our mixture. the hot plate set to med high. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Return to hot Rinsing with distilled water, then methanol, then distilled water again has been shown to work well. 60's with antihistamine or the time release type. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. contents of the beaker into the filter funnel and let drain. Add NaOH solution to water/pseudo/toluene funnel. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. When drying the cornstarch will keep our dissolve other substances which are not as readily soluble in the alcohol as the beaker. percent range. sucrose the used naptha filtering out free base crystals using a beaker on hot plate. for our solubility purposes. The near-universality of this procedure is its great advantage. 12) Heat dried ISO alcohol to boiling. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. The mixture will slowly thicken to a Xylene and Tolulene will, as will odorless mineral spirits. method now, but study Jacked's first so you really Get the RVessel the fuck outside or to a fire safe place. vapor, reduce the risk of fire and explosion. if you are going to do an RP/I2 or hypo cook. The process provided by. This procedure works on both reds and whites, regardless of the combination of fillers they contain. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel As with all pill extraction, the finer the pills are ground, the more likely Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Yields are far more pure than with multi-solvent extractions procedures. Take 4 by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Bottom Line. Acetone used for this purpose should be Advantages and Disadvantages: The increased solubility at higher temperatures Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. evaporated. and our Boil for 5 mins and then filter. Now you can either, evaporate toluene now for freebase crystals! Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017.
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